HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiomorpholine → HCID 11222563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiomorpholine | HCID 67164 | — |
| Reactant | HCID 86599257 | HCID 86599257 | — |
| Product | HCID 11222563 | HCID 11222563 | — |
Reaction Steps
The title compound was prepared (0.55 g, 39%) following the general procedure of Example 390 as a white solid, hydrochloride salt from (±)-([5-chloro-7-(2,6-dimethylphenyl)-2,3-dihydro-1-benzofuran-2-yl]methyl 4-methylbenzenesulfonate (0.15 g, 0.338 mmol) and thiomorpholine (0.72 g, 6.76 mmol). mp 224-226° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435837B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-8292ed26ccd347d5bce608b831db331e |
| Source note | uspto-grants-2008_10 |