HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 69108515, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 86599151 | HCID 86599151 | — |
| Product | HCID 69108515 | HCID 69108515 | — |
Reaction Steps
The title compound was prepared (0.068 g, 83%) following the general procedure of Example 390 as a white solid, hydrochloride salt from (±)-[7-(2,5-dichlorophenyl)-2,3-dihydro-1-benzofuran-2-yl]methyl 4-methylbenzenesulfonate (0.120 g, 0.26 mmol) and methylamine (1.24 g, 40.0 mmol). mp 147-149° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435837B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-1ecf65742e4542ea9ea3e0eeb6c7f6d1 |
| Source note | uspto-grants-2008_10 |