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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2116343Generated: October 30, 2026

Methylamine → HCID 68966216, compound

https://huagongshe.com/reaction/2116343

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethylamineHCID 6329—
ReactantHCID 86599308HCID 86599308—
ProductHCID 68966216HCID 68966216—

Reaction Steps

The title compound was prepared (0.046 g, 34%) following the general procedure of Example 390 as a white solid, hydrochloride salt from (±)-[5-chloro-7-(2,3-dimethoxyphenyl)-2,3-dihydro-1-benzofuran-2-yl]methyl 4-methylbenzenesulfonate (0.172 g, 0.36 mmol) and methylamine (0.112 g, 3.6 mmol). mp 105-107° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07435837B2
Source datasetuspto-grants-2008_10
ORD IDord-083315d625f24a989e1359745050feeb
Source noteuspto-grants-2008_10