HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methylamine → HCID 68964123, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methylamine | HCID 6329 | — |
| Reactant | HCID 86599329 | HCID 86599329 | — |
| Product | HCID 68964123 | HCID 68964123 | — |
Reaction Steps
The title compound was prepared (0.073 g, 78%) following the general procedure of Example 390 as a white solid, hydrochloride salt from (±)-[7-(2,6-dichlorophenyl) 5-methyl-2,3-dihydro-1-benzofuran-2-yl]methyl 4-methylbenzenesulfonate (0.12 g, 0.26 mmol) and methylamine (0.080 g, 2.6 mmol). mp 192-195° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07435837B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-95f49c533f3a4d9daf35395950b3d574 |
| Source note | uspto-grants-2008_10 |