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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2116368Generated: October 30, 2026

Methylamine → HCID 11961224, compound

https://huagongshe.com/reaction/2116368

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethylamineHCID 6329—
ReactantHCID 86599333HCID 86599333—
ProductHCID 11961224HCID 11961224—

Reaction Steps

The title compound was prepared (0.017 g, 18%) following the general procedure of Example 390 as a white solid, hydrochloride salt from (±)-{[7-(2,3-difluorophenyl)-5-methoxy-2,3-dihydro-1-benzofuran-2-yl]methyl}4-methylbenzenesulfonate (0.12 g, 0.27 mmol) and methylamine (0.082 g, 2.7 mmol). mp 148-150° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07435837B2
Source datasetuspto-grants-2008_10
ORD IDord-b0195e986ac4453397e16908a5c61f97
Source noteuspto-grants-2008_10