Sodium Cyanide → HCID 11779467, compound

Participants

Reaction Steps

A mixture of the product from step (iv) (0.13 g) and sodium cyanide (0.054 g) in dimethylsulphoxide (3 ml) was stirred at room temperature for 72 h then partitioned between ethyl acetate and water. The organic layer was washed with water, dried (MgSO4), evaporated under reduced pressure and the residue purified by chromatography on silica eluting with 2:1 ethyl acetate in isohexane. Yield 0.035 g

Provenance & Evidence