HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-methoxybenzene-1-sulfonyl chloride → HCID 9850299, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-methoxybenzene-1-sulfonyl chloride | HCID 520020 | — |
| Reactant | HCID 9948021 | HCID 9948021 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 9850299 | HCID 9850299 | 20.4% |
Reaction Steps
To a solution of the aniline produced in Example 1 (250 mg, 0.85 mmol) in CH2Cl2 (4 mL) was added 5-bromo-2-methoxybenzenesulfonyl chloride (244,mg, 0.85 mmol). The mixture was stirred for 10 hr. The title compound (94 mg, 20% to) was isolated following column chromatography on silica gel (1:1 hexane/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07439242B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-65d000ff43ee489b92761eaa309d4ab0 |
| Source note | uspto-grants-2008_10 |