(Diethylamino)trimethylsilane → HCID 86613024, compound

Participants

Reaction Conditions

Reaction Steps

0.62 g (4.27 mmol) of N,N-diethyltrimethylsilylamine are added over the course of a few minutes at room temperature with stirring to 1.0 g (3.54 mmol) of 1,3-dimethyl-2-chloroimidazolidinium trifluoromethanesulfonate in 15 ml of chloroform. The reaction mixture is stirred for 30 minutes at room temperature and for 30 minutes at 40-50° C. The volatile constituents are distilled off, and the residue obtained is dried at 50° C. under reduced pressure (7.0 Pa), giving 1.11 g of 1,3-dimethyl-2-diethylaminoimidazolidinium trifluoromethanesulfonate as an oil, corresponding to a yield of 98.2%.

Provenance & Evidence