HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 178483694, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 1,1-Dichloro-N,N,N',N'-tetramethylmethanediamine | HCID 12544745 | — |
| Product | HCID 178483694 | HCID 178483694 | 96.3% |
Reaction Steps
2.1 g (18.4 mmol) of trifluoroacetic acid are added with stirring to 3.0 g (17.5 mmol) of bis(dimethylamino)dichloromethane. The reaction is stirred for one hour at room temperature, and all volatile products are subsequently removed under reduced pressure at 7 Pa and 60° C., giving 4.19 g of bis(dimethylamino)chlorocarbenium trifluoroacetate as a very viscous oil, corresponding to a yield of 96.1%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07439395B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-8883ca33d79b401a86ce26aa746ac6f7 |
| Source note | uspto-grants-2008_10 |