HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → HCID 69317206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | Methyl 2-amino-6-chlorobenzoate | HCID 592849 | — |
| Reactant | HCID 178418573 | HCID 178418573 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 69317206 | HCID 69317206 | 89% |
Reaction Steps
This compound was prepared using General Method 1 (EXAMPLE 1) from methyl 2-amino-6-chlorobenzoate (1.7 g, 9.2 mmol) and methyl magnesium bromide (3 M in diethyl ether, 12.2 mL) in 45 mL ether to afford 1.5 g (89%) of 2-(2-amino-6-chlorophenyl)propan-2-ol after flash chromatography (5:3 hexanes:ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442696B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-0d43fdcd08e34af7928c775d3ef29e9f |
| Source note | uspto-grants-2008_10 |