HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
2-Amino-6-chlorobenzaldehyde → 1-(2-Amino-6-chlorophenyl)propan-1-ol
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 2-Amino-6-chlorobenzaldehyde | HCID 22399512 | — |
| Edukt | HCID 178418443 | HCID 178418443 | — |
| Lösungsmittel | Ethyl Acetate | HCID 8857 | — |
| Produkt | 1-(2-Amino-6-chlorophenyl)propan-1-ol | HCID 69318120 | 48% |
Reaktionsschritte
This compound was prepared using General Method 1 (EXAMPLE 1) from 2-amino-6-chlorobenzaldehyde (0.30 g, 1.9 mmol) and ethyl magnesium bromide (3 M in diethyl ether, 1.3 mL) to afford 0.17 g (48%) of (±)-1-(2-amino-6-chlorophenyl)propan-1-ol after flash chromatography (4:1 hexanes:ethyl acetate).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US07442696B2 |
| Quelldatensatz | uspto-grants-2008_10 |
| ORD ID | ord-49a6a2b9634a4783872f00be4e8c7dfa |
| Quellennotiz | uspto-grants-2008_10 |