HCID 11239513, compound → HCID 11260351, compound

Participants

Reaction Steps

To a solution of the product from Step 4 (130 mg, 0.18 mmol, 1.00 eq.) in methanol (0.5 mL) is added 10% Pd/C (20 mg, 0.02 mmol, 0.10 eq.). The reaction vessel is purged with H2 and then maintained under H2 via a balloon. The reaction is stirred under H2 overnight and then filtered and concentrated in vacuo yielding the product as a white solid (63 mg, 71% crude yield). Calculate mass for C26H36FN3O5: 489.26. Mass found for C26H36FN3O5: (OAMS) ES+: 489.8 (M+1), ES− 487.8 (M−1).

Provenance & Evidence