Chloroacetone → HCID 12069552, compound

HRID 2117364Notes

Reaction equation

HRID 2117364 reaction equation
[CH2:1]([N:8]([CH3:16])[CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][N:11]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Cl[CH2:18][C:19](=O)[CH3:20]>>[CH2:1]([N:8]([CH3:16])[C:9]1[C:19]([CH3:20])=[CH:18][N:11]2[C:10]=1[CH:15]=[CH:14][CH:13]=[CH:12]2)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 6571ChloroacetoneHCID 783552HCID 783552, compound

Product 1

HCID 12069552HCID 12069552, compoundYield 34%

Procedure

This compound is obtained according to the same procedure as the compound of Preparation I, using the Tschitschibabin reaction and starting with 2.47 g of N-benzyl-N-methyl-N-[(pyridin-2-yl)methyl]amine and chloroacetone. 970 mg of a yellow oil are obtained.

Workup

  1. customThis compound is obtained
  2. customaccording to the same procedure as the compound of Preparation I
  3. customthe Tschitschibabin reaction

Sources & evidence

ORD record
ord-e59c337b143f4f7a9ca5f00faeed4aa7
Source dataset
uspto-grants-2008_10
Patent number
US07442708B2

Reaction notes

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