Acetic Anhydride → HCID 68710035, compound

HRID 2117370Notes

Reaction equation

HRID 2117370 reaction equation
[C:1](OC(=O)C)(=[O:3])[CH3:2].[NH2:8][C:9]1[C:10]([CH3:31])=[C:11]([C:18]([C:20]2[CH:25]=[CH:24][C:23]([N+:26]([O-:28])=[O:27])=[C:22]([O:29][CH3:30])[CH:21]=2)=[O:19])[N:12]2[C:17]=1[CH:16]=[CH:15][CH:14]=[CH:13]2>ClCCl>[CH3:30][O:29][C:22]1[CH:21]=[C:20]([CH:25]=[CH:24][C:23]=1[N+:26]([O-:28])=[O:27])[C:18]([C:11]1[N:12]2[C:17]([CH:16]=[CH:15][CH:14]=[CH:13]2)=[C:9]([NH:8][C:1](=[O:3])[CH3:2])[C:10]=1[CH3:31])=[O:19]

Participants

4

Reactant 2

HCID 7918Acetic AnhydrideHCID 12069573HCID 12069573, compound

Product 1

HCID 68710035HCID 68710035, compound

Reagents, catalysts & solvents 1

HCID 6344DichloromethaneSolvent

Procedure

1.20 ml (12.60 mmol) of acetic anhydride are added to 410 mg (1.26 mmol) of (1-amino-2-methylindolizin-3-yl)(3-methoxy-4-nitrophenyl)methanone dissolved in 10 ml of dichloromethane.

Sources & evidence

ORD record
ord-2e0776d3554d4ec3885a5230524a6368
Source dataset
uspto-grants-2008_10
Patent number
US07442708B2

Reaction notes

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