2-Isopropoxy-5-methylsulfonylbenzoic acid → HCID 58677884, compound

HRID 2117420Notes

Reaction equation

HRID 2117420 reaction equation
[CH3:1][N:2]1[CH2:7][CH2:6][N:5]([S:8]([C:11]2[CH:20]=[C:19]3[C:14]([CH2:15][CH2:16][NH:17][CH2:18]3)=[CH:13][CH:12]=2)(=[O:10])=[O:9])[CH2:4][CH2:3]1.[CH:21]([O:24][C:25]1[CH:33]=[CH:32][C:31]([S:34]([CH3:37])(=[O:36])=[O:35])=[CH:30][C:26]=1[C:27](O)=[O:28])([CH3:23])[CH3:22]>>[CH:21]([O:24][C:25]1[CH:33]=[CH:32][C:31]([S:34]([CH3:37])(=[O:36])=[O:35])=[CH:30][C:26]=1[C:27]([N:17]1[CH2:16][CH2:15][C:14]2[C:19](=[CH:20][C:11]([S:8]([N:5]3[CH2:6][CH2:7][N:2]([CH3:1])[CH2:3][CH2:4]3)(=[O:10])=[O:9])=[CH:12][CH:13]=2)[CH2:18]1)=[O:28])([CH3:23])[CH3:22]

Participants

3

Reactant 2

HCID 211002372-Isopropoxy-5-methylsulfonylbenzoic acidHCID 28263248HCID 28263248, compound

Product 1

HCID 58677884HCID 58677884, compound

Procedure

Prepared in analogy to example 1.1 from 7-(4-methyl-piperazine-1-sulfonyl)-1,2,3,4-tetrahydro-isoquinoline (CA [741674-53-3]) and 2-isopropoxy-5-methanesulfonyl-benzoic acid (Example 2.1). MS (m/e): 536.3 (M+H+).

Sources & evidence

ORD record
ord-2817ad1d15454fb7a42b22dd8409c410
Source dataset
uspto-grants-2008_10
Patent number
US07442710B2

Reaction notes

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