33332-07-9 → HCID 58677877, compound

HRID 2117426Notes

Reaction equation

HRID 2117426 reaction equation
[O:1]1[C:13]2[C:12]3[CH2:11][NH:10][CH2:9][CH2:8][C:7]=3[CH:6]=[CH:5][C:4]=2[O:3][CH2:2]1.[CH:14]([O:17][C:18]1[CH:26]=[CH:25][C:24]([S:27]([CH3:30])(=[O:29])=[O:28])=[CH:23][C:19]=1[C:20](O)=[O:21])([CH3:16])[CH3:15]>>[O:1]1[C:13]2[C:12]3[CH2:11][N:10]([C:20]([C:19]4[CH:23]=[C:24]([S:27]([CH3:30])(=[O:29])=[O:28])[CH:25]=[CH:26][C:18]=4[O:17][CH:14]([CH3:16])[CH3:15])=[O:21])[CH2:9][CH2:8][C:7]=3[CH:6]=[CH:5][C:4]=2[O:3][CH2:2]1

Participants

3

Reactant 2

HCID 3641433332-07-9HCID 211002372-Isopropoxy-5-methylsulfonylbenzoic acid

Product 1

HCID 58677877HCID 58677877, compound

Procedure

Prepared in analogy to example 1.1 from 6,7,8,9-tetrahydro-[1,3]dioxolo [4,5-h]isoquinoline (CA [87091-23-4]) and 2-isopropoxy-5-methanesulfonyl-benzoic acid (Example 2.1). MS (m/e): 418.1 (M+H+).

Sources & evidence

ORD record
ord-df6399290e1640b5a624fac4b37c78c8
Source dataset
uspto-grants-2008_10
Patent number
US07442710B2

Reaction notes

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