2-Isopropoxy-5-methylsulfonylbenzoic acid → HCID 58677883, compound

HRID 2117443Notes

Reaction equation

HRID 2117443 reaction equation
[CH3:1][O:2][C:3]1[C:12]2[O:13][CH2:14][O:15][C:11]=2[C:10]2[CH2:9][NH:8][CH2:7][CH2:6][C:5]=2[CH:4]=1.[CH:16]([O:19][C:20]1[CH:28]=[CH:27][C:26]([S:29]([CH3:32])(=[O:31])=[O:30])=[CH:25][C:21]=1[C:22](O)=[O:23])([CH3:18])[CH3:17]>>[CH:16]([O:19][C:20]1[CH:28]=[CH:27][C:26]([S:29]([CH3:32])(=[O:31])=[O:30])=[CH:25][C:21]=1[C:22]([N:8]1[CH2:7][CH2:6][C:5]2[CH:4]=[C:3]([O:2][CH3:1])[C:12]3[O:13][CH2:14][O:15][C:11]=3[C:10]=2[CH2:9]1)=[O:23])([CH3:18])[CH3:17]

Participants

3

Reactant 2

HCID 211002372-Isopropoxy-5-methylsulfonylbenzoic acidHCID 57445272HCID 57445272, compound

Product 1

HCID 58677883HCID 58677883, compound

Procedure

Prepared in analogy to example 1.1 from 4-methoxy-6,7,8,9-tetrahydro-[1,3]dioxolo[4,5-h]isoquinoline (CA [110103-21-4]) and 2-isopropoxy-5-methanesulfonyl-benzoic acid (Example 2.1). MS (m/e): 448.3 (M+H+).

Sources & evidence

ORD record
ord-13755fe884df4440a2447b97de17855a
Source dataset
uspto-grants-2008_10
Patent number
US07442710B2

Reaction notes

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