2-Isopropoxy-5-methylsulfonylbenzoic acid → HCID 11719257, compound

HRID 2117444Notes

Reaction equation

HRID 2117444 reaction equation
[CH3:1][C:2]1[C:11]2[CH2:10][NH:9][CH2:8][CH2:7][C:6]=2[C:5]([CH3:12])=[C:4]2[O:13][CH2:14][O:15][C:3]=12.[CH:16]([O:19][C:20]1[CH:28]=[CH:27][C:26]([S:29]([CH3:32])(=[O:31])=[O:30])=[CH:25][C:21]=1[C:22](O)=[O:23])([CH3:18])[CH3:17]>>[CH3:1][C:2]1[C:11]2[CH2:10][N:9]([C:22]([C:21]3[CH:25]=[C:26]([S:29]([CH3:32])(=[O:31])=[O:30])[CH:27]=[CH:28][C:20]=3[O:19][CH:16]([CH3:18])[CH3:17])=[O:23])[CH2:8][CH2:7][C:6]=2[C:5]([CH3:12])=[C:4]2[O:13][CH2:14][O:15][C:3]=12

Participants

3

Reactant 2

HCID 211002372-Isopropoxy-5-methylsulfonylbenzoic acidHCID 57445273HCID 57445273, compound

Product 1

HCID 11719257HCID 11719257, compound

Procedure

Prepared in analogy to example 1.1 from 4,9-dimethyl-5,6,7,8-tetrahydro-[1,3]dioxolo[4,5-g]isoquinoline and 2-isopropoxy-5-methanesulfonyl-benzoic acid (Example 2.1). MS (m/e): 446.3 (M+H+).

Sources & evidence

ORD record
ord-a4a421d396244dfb96bd7f3e595dbdd1
Source dataset
uspto-grants-2008_10
Patent number
US07442710B2

Reaction notes

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