6-Methyl-1,2,3,4-tetrahydroquinoline → HCID 58677902, compound

HRID 2117452Notes

Reaction equation

HRID 2117452 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[NH:8][CH2:7][CH2:6][CH2:5]2.[CH:12]([O:15][C:16]1[CH:24]=[CH:23][C:22]([S:25]([CH3:28])(=[O:27])=[O:26])=[CH:21][C:17]=1[C:18](O)=[O:19])([CH3:14])[CH3:13]>CC(O)=O>[CH:12]([O:15][C:16]1[CH:24]=[CH:23][C:22]([S:25]([CH3:28])(=[O:27])=[O:26])=[CH:21][C:17]=1[C:18]([N:8]1[C:9]2[C:4](=[CH:3][C:2]([CH3:1])=[CH:11][CH:10]=2)[CH2:5][CH2:6][CH2:7]1)=[O:19])([CH3:14])[CH3:13]

Participants

4

Reactant 2

HCID 666786-Methyl-1,2,3,4-tetrahydroquinolineHCID 211002372-Isopropoxy-5-methylsulfonylbenzoic acid

Product 1

HCID 58677902HCID 58677902, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

Prepared in analogy to example 1.1 from 6-methyl-1,2,3,4-tetrahydro-quinoline (CA [91-61-2]) and 2-isopropoxy-5-methanesulfonyl-benzoic acid (Example 2.1). MS (m/e): 445.9 (M+CH3COOH).

Sources & evidence

ORD record
ord-3dd4120acbcf4f81a57727c145d4ef24
Source dataset
uspto-grants-2008_10
Patent number
US07442710B2

Reaction notes

Loading…