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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2117661Generated: October 31, 2026

Ammonia → HCID 21895619, compound

https://huagongshe.com/reaction/2117661

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAmmoniaHCID 222—
ReactantHCID 15118080HCID 15118080—
SolventTetrahydrofuranHCID 8028—
ProductHCID 21895619HCID 21895619—

Reaction Steps

A stirred solution of (3-iodophenyl)methanesulfonyl chloride (1 g) in THF (20 ml) was treated with 0.88 ammonia (25 ml) at room temperature for 30 min. The solvent was removed under reduced pressure and the residue was triturated in ether to give the title compound (0.35 g). LCMS RT=2.71 min.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07442719B2
Source datasetuspto-grants-2008_10
ORD IDord-8c29858141e74353b03bbb7f33944195
Source noteuspto-grants-2008_10