HRID2117666

反应详情

EQUATION

反应方程式

HRID 2117666 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of 4-(3-bromophenyl)but-3-yn-1-ol (21 g) in ethanol (1000 ml) was hydrogenated over platinum oxide (500 mg) for 4 h. The catalyst was removed by filtration and the filtrate was evaporated to give the title compound (18 g) tlc (SiO2) diethyl ether Rf=0.38.

WORKUP

后处理

  1. customThe catalyst was removed by filtration
  2. customthe filtrate was evaporated