Cyanuric chloride → HCID 59010023, compound

Participants

Reaction Steps

To a stirred solution of the corresponding amide (Example 21, 386 mg, 0.96 mmol) in DMF (5 mL) was added cyanuric chloride (89 mg, 0.48 mmol). The reaction was stirred at room temperature for 2h. After aqueous workup, the crude product was purified on a silica gel column, eluting with ethyl acetate (0-30%) in hexanes. The final product was collected as colorless oil.

Provenance & Evidence