HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl L-phenylalaninate hydrochloride → Ethyl N-[(5-amino-1-methyl-3-phenyl-1H-indol-2-yl)carbonyl]-L-phenylalaninate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl L-phenylalaninate hydrochloride | HCID 165085 | — |
| Reactant | 1-Methyl-5-nitro-3-phenyl-1H-indole-2-carboxylic acid | HCID 21543518 | — |
| Product | Ethyl N-[(5-amino-1-methyl-3-phenyl-1H-indol-2-yl)carbonyl]-L-phenylalaninate | HCID 69228463 | — |
Reaction Steps
Ethyl N-[(5-amino-1-methyl-3-phenyl-1H-indol-2-yl)carbonyl]-L-phenylalaninate was prepared from 1-methyl-5-nitro-3-phenyl-1H-indole-2-carboxylic acid and L-phenylalanine ethyl ester hydrochloride followed the procedure of Example 8 Step 2 as a pale yellow solid: MS (ESI) m/z 442 (MH+); HRMS calcd for C27H28N3O3: 442.2128; found (ESI+): 442.2122.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442805B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-1f85226ef43d4425b37c021a8483c6e5 |
| Source note | uspto-grants-2008_10 |