Benzenesulfonyl chloride → HCID 11432932, compound

Participants

Reaction Steps

The title compound was prepared from ethyl 5-amino-1-benzhydryl-3-phenyl-1H-indole-2-carboxylate and phenylsulfonyl chloride followed the procedure of Example 1 Step 3 as a pale yellow solid: 1H NMR (DMSO-d6) δ 6.68 (d, J=9.0 Hz, 1H, 6.78 (dd, J=9.2, 2.2 Hz, 1H), 7.04 (d, J=2.2 Hz, 1H, 7.13 (d, J=7.1 Hz, 4H, 7.25-7.30 (m, 2H, 7.30-7.40 (m, 7H, 7.40-7.55 (m, 4H, 7.58-7.68 (m, 3H, 7.84 (s, 1H, 9.93 (s, 1H, 13.19 (br s, 1H; MS (ESI) m/z 557 [M-H]−; HRMS calcd for C34H27N2O4S: 559.1689; found (ESI+): 559.1686; Anal. calcd for C34H26N2O4S.0.6H2O: C, 71.71; H, 4.81; N, 4.92. Found: C, 71.51; H, 4.77; N, 5.11.

Provenance & Evidence