HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 21895619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | HCID 15118080 | HCID 15118080 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 21895619 | HCID 21895619 | — |
Reaction Steps
A stirred solution of (3-iodophenyl)methanesulfonyl chloride (1 g) in THF (20 ml) was treated with 0.88 ammonia (25 ml) at room temperature for 30 min. The solvent was removed under reduced pressure and the residue was triturated in ether to give the title compound (0.35 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07442837B2 |
| Source dataset | uspto-grants-2008_10 |
| ORD ID | ord-8afb56b66ca042bb98f18dceef561e0c |
| Source note | uspto-grants-2008_10 |