Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2118353Generated: October 31, 2026

HCID 69119808, compound → HCID 10098658, compound

https://huagongshe.com/reaction/2118353

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 69119808HCID 69119808—
CatalystPalladiumHCID 23938—
SolventAcetic AcidHCID 176—
SolventEthyl AcetateHCID 8857—
ProductHCID 10098658HCID 10098658—

Reaction Steps

To an evacuated flask containing palladium on carbon [50% water by weight] was added a solution of (1R)-2-{[6-({4-[3-(cyclopentylsulfonyl)phenyl]butyl}oxy)hexyl]amino)-1-{3-fluoro-4-[(phenylmethyl)oxy]phenyl}ethanol (37 mg) in EtOAc (8 ml) and AcOH (2 ml). The reaction mixture was hydrogenated for 4 h. The catalyst was filtered off and the filtrate concentrated in vacuo to give the title compound. LCMS RT=2.60 min 535(M+H)+

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07442839B2
Source datasetuspto-grants-2008_10
ORD IDord-03fe939cfadd4b37aa03408d4491543e
Source noteuspto-grants-2008_10