Thionyl Chloride → HCID 21982108, compound

HRID 2118369Notes

Reaction equation

HRID 2118369 reaction equation
[CH2:1]([C:9]1([CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[C:21]2[CH:20]=[C:19]([C:22](O)=[O:23])[CH:18]=[CH:17][C:16]=2[C:15]2[C:10]1=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8].S(Cl)([Cl:35])=O>>[CH2:1]([C:9]1([CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][CH2:30][CH2:31][CH3:32])[C:21]2[CH:20]=[C:19]([C:22]([Cl:35])=[O:23])[CH:18]=[CH:17][C:16]=2[C:15]2[C:10]1=[CH:11][CH:12]=[CH:13][CH:14]=2)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH3:8]

Participants

3

Reactant 2

HCID 24386Thionyl Chloride2×HCID 219820809,9-Dioctyl-9H-fluorene-2-carboxylic Acid

Product 1

HCID 21982108HCID 21982108, compound

Procedure

9,9-Dioctyl-9H-fluorene-2-carboxylic acid (32.36 g, 74.5 mmole) was refluxed in thionyl chloride (93 g, 782 mmole) for 8 hrs. Unreacted thionyl chloride was distilled off and the residue material used without further purification.

Workup

  1. distillationwas distilled off
  2. customthe residue material used without further purification

Sources & evidence

ORD record
ord-550db120cef641798b91b2e00dabf534
Source dataset
uspto-grants-2008_10
Patent number
US07442760B2

Reaction notes

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