2-Chlorobenzyl chloride → HCID 20194020, compound

HRID 2118506Notes

Reaction equation

HRID 2118506 reaction equation
[CH3:1][C:2]1[CH:11]=[CH:10][CH:9]=[C:8]2[C:3]=1[CH2:4][CH2:5][N:6]=[CH:7]2.[Cl:12][C:13]1[CH:20]=[CH:19][CH:18]=[CH:17][C:14]=1[CH2:15]Cl>O1CCOCC1>[Cl-:12].[Cl:12][C:13]1[CH:20]=[CH:19][CH:18]=[CH:17][C:14]=1[CH2:15][N+:6]1[CH2:5][CH2:4][C:3]2[C:8](=[CH:9][CH:10]=[CH:11][C:2]=2[CH3:1])[CH:7]=1

Participants

4

Reactant 2

HCID 119062-Chlorobenzyl chlorideHCID 19748115HCID 19748115, compound

Product 1

HCID 20194020HCID 20194020, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

The title compound is prepared analogously to Example A from 5-methyl-3,4-dihydro-isoquinoline and 2-chlorobenzyl chloride in dioxan. Melting point: 166°-168° C.

Sources & evidence

ORD record
ord-82de4e65b4274365b6d902a49d99cd78
Source dataset
uspto-grants-1987_07
Patent number
US04678792

Reaction notes

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