2-Chlorobenzyl chloride → HCID 13562950, compound

HRID 2118507Notes

Reaction equation

HRID 2118507 reaction equation
[CH3:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][C:11]=1[CH3:12])[CH:8]=[N:7][CH2:6][CH2:5]2.[Cl:13][C:14]1[CH:21]=[CH:20][CH:19]=[CH:18][C:15]=1[CH2:16]Cl>O1CCOCC1>[Cl-:13].[Cl:13][C:14]1[CH:21]=[CH:20][CH:19]=[CH:18][C:15]=1[CH2:16][N+:7]1[CH2:6][CH2:5][C:4]2[C:9](=[CH:10][C:11]([CH3:12])=[C:2]([CH3:1])[CH:3]=2)[CH:8]=1

Participants

4

Reactant 2

HCID 119062-Chlorobenzyl chlorideHCID 13562943HCID 13562943, compound

Product 1

HCID 13562950HCID 13562950, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

The title compound is prepared analogously to Example A from 6,7-dimethyl-3,4-dihydroisoquinoline and 2-chlorobenzyl chloride in dioxan. Melting point: 127°-129° C.

Sources & evidence

ORD record
ord-cd2c75d55c744b16b02362feb0b9e253
Source dataset
uspto-grants-1987_07
Patent number
US04678792

Reaction notes

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