Benzyl Chloride → HCID 13562954, compound

HRID 2118509Notes

Reaction equation

HRID 2118509 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][C:12]=1[O:13][CH3:14])[CH:9]=[N:8][CH2:7][CH2:6]2.[CH2:15]([Cl:22])[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>O1CCOCC1>[Cl-:22].[CH2:15]([N+:8]1[CH2:7][CH2:6][C:5]2[C:10](=[CH:11][C:12]([O:13][CH3:14])=[C:3]([O:2][CH3:1])[CH:4]=2)[CH:9]=1)[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 7503Benzyl ChlorideHCID 300583,4-Dihydro-6,7-dimethoxyisoquinoline

Product 1

HCID 13562954HCID 13562954, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

The title compound is prepared analogously to Example A from 6,7-dimethoxy-3,4-dihydroisoquinoline and benzyl chloride in dioxan. The melting point: 181°-183° C. (Decomp.)

Sources & evidence

ORD record
ord-b01233f6390b4a3da1418361eaadc85a
Source dataset
uspto-grants-1987_07
Patent number
US04678792

Reaction notes

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