alpha-Chloro-o-xylene → HCID 13562955, compound

HRID 2118511Notes

Reaction equation

HRID 2118511 reaction equation
[CH3:1][O:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][C:12]=1[O:13][CH3:14])[CH:9]=[N:8][CH2:7][CH2:6]2.[CH3:15][C:16]1[CH:23]=[CH:22][CH:21]=[CH:20][C:17]=1[CH2:18][Cl:19]>O1CCOCC1>[Cl-:19].[CH3:15][C:16]1[CH:23]=[CH:22][CH:21]=[CH:20][C:17]=1[CH2:18][N+:8]1[CH2:7][CH2:6][C:5]2[C:10](=[CH:11][C:12]([O:13][CH3:14])=[C:3]([O:2][CH3:1])[CH:4]=2)[CH:9]=1

Participants

4

Reactant 2

HCID 11093alpha-Chloro-o-xyleneHCID 300583,4-Dihydro-6,7-dimethoxyisoquinoline

Product 1

HCID 13562955HCID 13562955, compound

Reagents, catalysts & solvents 1

HCID 312751,4-DioxaneSolvent

Procedure

The title compound is prepared analogously to Example A from 6,7-dimethoxy-3,4-dihydroisoquinoline and 2-methyl-benzyl chloride in dioxan. Melting point: 193°-195° C. (Decomp., from ethanol-ether).

Sources & evidence

ORD record
ord-32b8fc8ebea44de5a277a3fac8255dcf
Source dataset
uspto-grants-1987_07
Patent number
US04678792

Reaction notes

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