Acetyl chloride → p-[(E)-2-(4,4-dimethyl-6-chromanyl)propenyl]benzyl acetate

HRID 2118525Notes

Reaction equation

HRID 2118525 reaction equation
[CH3:1][C:2]1([CH3:23])[C:11]2[C:6](=[CH:7][CH:8]=[C:9](/[C:12](/[CH3:22])=[CH:13]/[C:14]3[CH:21]=[CH:20][C:17]([CH2:18][OH:19])=[CH:16][CH:15]=3)[CH:10]=2)[O:5][CH2:4][CH2:3]1.[C:24](Cl)(=[O:26])[CH3:25]>N1C=CC=CC=1>[C:24]([O:19][CH2:18][C:17]1[CH:16]=[CH:15][C:14](/[CH:13]=[C:12](/[C:9]2[CH:10]=[C:11]3[C:6](=[CH:7][CH:8]=2)[O:5][CH2:4][CH2:3][C:2]3([CH3:23])[CH3:1])\[CH3:22])=[CH:21][CH:20]=1)(=[O:26])[CH3:25]

Participants

4

Reactant 2

HCID 6367Acetyl chlorideHCID 13478154p-[(E)-2-(4,4-dimethyl-6-chromanyl)propenyl]benzyl alcohol

Product 1

HCID 70420679p-[(E)-2-(4,4-dimethyl-6-chromanyl)propenyl]benzyl acetate

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

By treating p-[(E)-2-(4,4-dimethyl-6-chromanyl)propenyl]benzyl alcohol with acetyl chloride and pyridine there is obtained p-[(E)-2-(4,4-dimethyl-6-chromanyl)propenyl]benzyl acetate.

Sources & evidence

ORD record
ord-21f39b0a86ff44a0a86ca219bee86998
Source dataset
uspto-grants-1987_07
Patent number
US04678793

Reaction notes

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