HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylhydroxylamine → N-n-Octadecyl-3-[(N,N-dibenzylamino)oxy]pyrrolidine-2,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylhydroxylamine | HCID 69297 | — |
| Reactant | 1-octadecyl-1H-pyrrole-2,5-dione | HCID 87118 | — |
| Product | N-n-Octadecyl-3-[(N,N-dibenzylamino)oxy]pyrrolidine-2,5-dione | HCID 14224083 | — |
Reaction Steps
The procedure of Example 1 is repeated using 6.10 g (29 mmole) of N,N-dibenzylhydroxylamine and 10.0 g (29 mmole) of N-n-octadecylmaleimide. The residue is purified by preparative HPLC (Silica gel: 9:1 heptane:ethyl acetate eluent) to give 8.0 g (49%) of a waxy solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04678826 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-0b85d6a48ba1415095c7ab32c6b3787b |
| Source note | uspto-grants-1987_07 |