HuagongsheHuagongshe Chemistry Print Report · For research reference only
Maleimide → HCID 14224080, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Maleimide | HCID 10935 | — |
| Reactant | Dibenzylhydroxylamine | HCID 69297 | — |
| Product | HCID 14224080 | HCID 14224080 | 74% |
Reaction Steps
The procedure of Example 1 is repeated using 5.33 g (25 mmole) of N,N-dibenzylhydroxylamine and 2.42 g (25 mmole) of maleimide. The residue is purified by preparative HPLC (Silica gel: 4:1 heptane:ethyl acetate eluent) to give 5.4 g (74%) of a colorless gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04678826 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-599702cce3184f099ba88a7212cb9ed5 |
| Source note | uspto-grants-1987_07 |