HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 12772315, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | 2-Amino-4-chloropyridine | HCID 581866 | — |
| Product | HCID 12772315 | HCID 12772315 | — |
Reaction Steps
The starting material was obtained by allowing a mixture of 2-amino-4-chloropyridine and excess methyl iodide (no solvent) to stand at ambient temperature for 2 days to give 2-amino-4-chloro-1-methylpyridinium iodide as a solid, n.m.r. in d6DMSO: 3.6(s, 3H); 6.6-6.7(m, 1H); 7.0(d, 1H); 7.9(d, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04678781 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-cc442b3280f542ac9f6c5fb504ad3270 |
| Source note | uspto-grants-1987_07 |