HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromoisoquinoline → 1-Bromo-2-methylisoquinolinium tetrafluoroborate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromoisoquinoline | HCID 640963 | — |
| Reactant | Oxonium, trimethyl-, tetrafluoroborate(1-) (1:1) | HCID 2735153 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 1-Bromo-2-methylisoquinolinium tetrafluoroborate | HCID 20028971 | — |
Reaction Steps
The starting material was prepared by reaction of 1-bromoisoquinoline with trimethyloxonium tetrafluoroborate in CH2Cl2 to give 1-bromo-2-methylisoquinolinium tetrafluoroborate, m.p. 162°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04678781 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-ac0fd97dbf8d414f8bd35fe6df3a2149 |
| Source note | uspto-grants-1987_07 |