HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 88657694, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 10022430 | HCID 10022430 | — |
| Product | HCID 88657694 | HCID 88657694 | 103% |
Reaction Steps
Boc-D-Met-Leu-OCH3 (25 g, 66.5 mmol) was dissolved in methyl iodide (132 ml) and stirred at room temperature for 2 days. Concentration in vacuo gave 35.4 g (103%) of the sulfonium salt. The nmr spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680283 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-73f45ec087d64ade89582b65d54774be |
| Source note | uspto-grants-1987_07 |