5-Chloroisatoic anhydride → 2-Amino-5-chloro-N-[3-(1H-1,2,4-triazol-1-yl)propyl]benzamide

HRID 2118649Notes

Reaction equation

HRID 2118649 reaction equation
[Cl:1][C:2]1[CH:13]=[C:6]2[C:7]([O:9]C(=O)[NH:11][C:5]2=[CH:4][CH:3]=1)=O.[N:14]1([CH2:19][CH2:20][CH2:21][NH2:22])[CH:18]=[N:17][CH:16]=[N:15]1>>[NH2:11][C:5]1[CH:4]=[CH:3][C:2]([Cl:1])=[CH:13][C:6]=1[C:7]([NH:22][CH2:21][CH2:20][CH2:19][N:14]1[CH:18]=[N:17][CH:16]=[N:15]1)=[O:9]

Participants

3

Reactant 2

HCID 784805-Chloroisatoic anhydrideHCID 43796821H-1,2,4-Triazole-1-propanamine

Product 1

HCID 135888972-Amino-5-chloro-N-[3-(1H-1,2,4-triazol-1-yl)propyl]benzamide

Procedure

When 5-chloroisatoic anhydride was reacted with 3-(1H-1,2,4-triazol-1-yl)propylamine by the procedure of Example 14, this compound, mp 116°-118° C., was obtained.

Workup

  1. customthis compound, mp 116°-118° C., was obtained

Sources & evidence

ORD record
ord-1c2a67c965024763b0a1028b858f6f2f
Source dataset
uspto-grants-1987_07
Patent number
US04680293

Reaction notes

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