Cyanogen Bromide → HCID 13957311, compound

HRID 2118669Notes

Reaction equation

HRID 2118669 reaction equation
[C:1]1([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][NH:20][C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[N:27]#[C:28]Br>C1C=CC=CC=1>[C:1]1([O:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][N:20]([C:21]2[CH:26]=[CH:25][CH:24]=[CH:23][CH:22]=2)[C:28]#[N:27])[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1

Participants

4

Reactant 2

HCID 10476Cyanogen BromideHCID 135205561-(1-Naphthyloxy)-8-(phenylamino)octane

Product 1

HCID 13957311HCID 13957311, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

4.5 g of 1-(1-naphthyloxy)-8-(phenylamino)octane and 1.4 g of cyanogen bromide were heated in 150 ml of benzene at 55° for 2 hours. The benzene was then evaporated from the solution, affording 1-(1-naphthyloxy)-8-(phenylcyanoamino)octane which was employed in Step B (below) without further purification.

Workup

  1. customThe benzene was then evaporated from the solution

Sources & evidence

ORD record
ord-ba2d838e48834c7e92cb9cd608a3f036
Source dataset
uspto-grants-1987_07
Patent number
US04680300

Reaction notes

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