Octadecylamine → HCID 18608592, compound

HRID 2118704Notes

Reaction equation

HRID 2118704 reaction equation
O=[CH:2][C@H:3]([C@@H:5]([C@@H:7]([C@H:9]([CH3:11])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:12]([NH2:30])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]>C(O)C>[CH2:12]([NH:30][CH:11]1[O:4][C@@H:3]([CH3:2])[C@@H:5]([OH:6])[C@@H:7]([OH:8])[C@@H:9]1[OH:10])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]

Participants

4

Reactant 2

HCID 15793OctadecylamineHCID 3034656L-(-)-Fucose

Product 1

HCID 18608592HCID 18608592, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

3.26 g of L-fucose and 5.38 g of stearylamine in 20 ml of ethanol are heated at 70° C., with stirring, until a clear solution has resulted. This is allowed to cool and, when crystallization is complete, the solid is filtered off with suction and washed with ethanol and ether.

Workup

  1. customhas resulted
  2. temperatureto cool
  3. customwhen crystallization
  4. filtrationthe solid is filtered off with suction
  5. washwashed with ethanol and ether

Sources & evidence

ORD record
ord-4e088cc5716a4b9aa1b1ec0fb7265c69
Source dataset
uspto-grants-1987_07
Patent number
US04680287

Reaction notes

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