HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20192951, compound → HCID 20192925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20192951 | HCID 20192951 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 20192925 | HCID 20192925 | — |
Reaction Steps
A solution of 173 g of 2-tert-butyl-5-[morpholin-4-yl]-6-nitrobenzothiazole in 5000 ml of methanol is hydrogenated in presence of 40 g of Raney Nickel at room temperature. After removing the catalyst the solution is concentrated and the solid filtered to give 6-amino-2-tert-butyl-5-morpholinobenzothiazole, melting at 158°-159°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680301 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-67abb415c5784f12a67eba4f371083d4 |
| Source note | uspto-grants-1987_07 |