関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Phthalic Anhydride | HCID 6811 | — |
| 反応物 | Hexahydrophthalic anhydride | HCID 85689 | — |
| 生成物 | Caprolactone acrylate | HCID 66599592 | — |
反応手順
An acid-terminated caprolactone acrylate was prepared by combining 37.0 g of phthalic anhydride, 19.25 g of hexahydrophthalic anhydride, and 129.0 g of TONE Monomer M-100 in a glass, four-neck reaction flask equipped with a stirrer, a thermometer, an air inlet and an air outlet, and heating them at 125° C. for 3.5 hours. The product was recovered and found to have an Acid Number of 114 and a viscosity of 1690 cp when measured at 25° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US04680361 |
|---|
| 出典データセット | uspto-grants-1987_07 |
|---|
| ORD ID | ord-9a4938125f1c4bea98acfbe799c2411e |
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| 出典メモ | uspto-grants-1987_07 |
|---|
