HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzenethiol → HCID 19748757, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzenethiol | HCID 15809 | — |
| Reactant | HCID 14543786 | HCID 14543786 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 19748757 | HCID 19748757 | — |
Reaction Steps
3-Propyl-4-acetoxy azetidinone, 171 mg, is refluxed with 200 mg p-nitrophenyl thiol in 10 ml benzene for 6 hours. The solution is washed 3x with aqueous Na2CO3, dried with MgSO4, filtered and evaporated. The residue is chromatographed on silica gel, eluting with 10:1 CHCl3 -EtOAc, affording 3-propyl-4-p-nitrophenylthioazetidin-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680391 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-cdb187ed9eb145cd8ddb01b124ef7621 |
| Source note | uspto-grants-1987_07 |