HuagongsheHuagongshe Chemistry Print Report · For research reference only
Calcium Carbonate → HCID 20193522, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Calcium Carbonate | HCID 10112 | — |
| Reactant | 3,5-Dimethylpiperidine | HCID 118259 | — |
| Reactant | (2-Chloro-5-nitro-phenyl)-(4-chloro-phenyl)-methanone | HCID 875720 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20193522 | HCID 20193522 | 98.1% |
Reaction Steps
Proceeding as indicated in example 2, with 0.035 mole (10.4 g) of 2,4'-dichloro-5-nitro-benzophenone, 0.07 mole (8 cm3) of 3,5-dimethylpiperidine and 0.035 mole (5 g) of calcium carbonate in ethanol, 12.8 g (Yield: 97%) of the expected product are obtained. M.P 159° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04680402 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-ab622437e7c44180bb95bf47a79e244a |
| Source note | uspto-grants-1987_07 |