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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2118876Generated: October 31, 2026

Sodium cyanoborohydride → HCID 18605797, compound

https://huagongshe.com/reaction/2118876

Reaction equation

Participants

RoleNameHCIDCharge
ReactantSodium cyanoborohydrideHCID 5003444—
ReactantHCID 11543093HCID 11543093—
ReactantHCID 18605799HCID 18605799—
SolventTriethylamineHCID 8471—
ProductHCID 18605797HCID 18605797—

Reaction Steps

React 1.08 g 3-(S)-amino-1-carboxymethylperhydroazepin-2-one hydrochloride, 5.3 g ethyl 2-oxo-5-phenylpentanoate, 0.49 g triethylamine and 630 mg sodium cyanoborohydride as described in Example 2. Purify the crude product by chromatography on LH 20 and isolate the desired ester.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04680392
Source datasetuspto-grants-1987_07
ORD IDord-dcb03d0aad63445d991109b5e60f1fb3
Source noteuspto-grants-1987_07