Sodium Methoxide → HCID 13914627, compound

Participants

Reaction Steps

A solution of 3.52 g (5.6 mmol) of 4-amino-3-bromo-1-(2,3,5-tri-O-benzoyl-β-D-ribofuranosyl)-2(1H)-pyridinone and 0.556 mmol of sodium methoxide in 50 ml of methanol was stirred at room temperature for 24 hours. At the end of this time, 0.88 g of methanol-washed IRC-50 ion exchange resin (Dow Chemical Co., Midland, Mich., USA) in the hydrogen ion form were added to the solution, and the resulting mixture was stirred for one hour.

Provenance & Evidence