HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2119008Generated: November 2, 2026
Potassium Carbonate → HCID 13689403, compound
https://huagongshe.com/reaction/2119008
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 11-(piperdin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine | HCID 13689358 | — |
| Reactant | HCID 54410630 | HCID 54410630 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 13689403 | HCID 13689403 | — |
Reaction Steps
A mixture of 11-(piperidin-4-yl)-5H,11H-pyrrolo[2,1-c][1,4]benzoxazepine (6.15 g, 0.023 mole), 2-(3-trifluoromethylphenyl)ethyl menthanesulfonate (7.27 g, 0.027 mole) and K2CO3 (10.6 g) in 125 ml dimethylformamide was heated at 65° C. for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04681879 |
|---|
| Source dataset | uspto-grants-1987_07 |
|---|
| ORD ID | ord-9d79d6c25a4f4e8aa90ae0099b4ba69a |
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| Source note | uspto-grants-1987_07 |
|---|
