Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 70431838 | HCID 70431838 | — |
| Product | HCID 13851473 | HCID 13851473 | — |
Reaction Steps
A mixture of [1-(4-chloro-2-fluorobenzyl)-2-pyrryl][(1-methyl)piperidin-4-yl]methanol (0.65 g, 0.002 mole) and sodium hydride (50% in oil, 0.12 g, 0.0023 mole, washed once with hexane) in 25 ml 20% DMF/benzene was heated at 80° C. for seven hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04681879 |
|---|
| Source dataset | uspto-grants-1987_07 |
|---|
| ORD ID | ord-71b6b4d12b92480091f875198a4d1d7f |
|---|
| Source note | uspto-grants-1987_07 |
|---|
