HuagongsheHuagongshe Chemistry Print Report · For research reference only
CID 70900 → HCID 13249025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | CID 70900 | HCID 70900 | — |
| Reactant | Tiglic acid | HCID 125468 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 13249025 | HCID 13249025 | 76.5% |
Reaction Steps
20.02 g (0.2 mol) of (E)-2-methyl-2-butenoic acid was dissolved in 100 ml of dry ethyl ether. 36.0 g (0.2 mol) of trichlorogermane was added to the solution and stirred for 2 hrs. Crystals thus formed were recrystallized from n-hexane to obtain 42.86 g (yield: 76.5%) of 2-methyl-3-(trichlorogermyl)butanoic acid in the form of colorless plate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04681960 |
| Source dataset | uspto-grants-1987_07 |
| ORD ID | ord-c0812c5604bf4192a3b9658f7863d8f1 |
| Source note | uspto-grants-1987_07 |