Octadecylamine → HCID 18608592, compound

HRID 2119149Notes

Reaction equation

HRID 2119149 reaction equation
O=[CH:2][C@H:3]([C@@H:5]([C@@H:7]([C@H:9]([CH3:11])[OH:10])[OH:8])[OH:6])[OH:4].[CH2:12]([NH2:30])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]>C(O)C>[CH2:12]([NH:30][CH:11]1[O:4][C@@H:3]([CH3:2])[C@@H:5]([OH:6])[C@@H:7]([OH:8])[C@@H:9]1[OH:10])[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]

Participants

4

Reactant 2

HCID 15793OctadecylamineHCID 3034656L-(-)-Fucose

Product 1

HCID 18608592HCID 18608592, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

3.26 g of L-fucose and 5.38 g of stearylamine in 20 ml of ethanol were heated to 70° C. with stirring until a clear solution had resulted. It was allowed to cool down and, after completion of crystallisation, the solid material was filtered off with suction and washed with ethanol and ether.

Workup

  1. customhad resulted
  2. temperatureto cool down
  3. customafter completion of crystallisation
  4. filtrationthe solid material was filtered off with suction
  5. washwashed with ethanol and ether

Sources & evidence

ORD record
ord-4e5b7ef305714ff68abe3bc7c11ab8f0
Source dataset
uspto-grants-1987_07
Patent number
US04683222

Reaction notes

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